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NWFSC Metadata Library > EFS (Environmental and Fisheries Sciences) Divi... > Lipophilic Toxins in WA - Clear and present dan... >

results from liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspi...

Entity (ENT)  |  Northwest Fisheries Science Center (NWFSC)
GUID: gov.noaa.nmfs.inport:54713  |  Updated: August 9, 2022  |  Published / External 
Summary
Item Identification
Entity Info
Data Attributes
Catalog Details

Summary

Abstract

Site names, coordinates, dates, and times that shellfish samples were collected for lipophilic marine toxin analyses. The results liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) are included. Additionally, the results of a screening assay for lipophilic toxins (PP2A) that detects okadaic acid and the dinophysis toxins are included.

Description

Site names, coordinates, dates, and times that shellfish samples were collected for lipophilic marine toxin analyses. The results liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) are included. Additionally, the results of a screening assay for lipophilic toxins (PP2A) that detects okadaic acid and the dinophysis toxins are included.

Entity Information

Entity Type
Spreadsheet

Data Attribute / Type Description
SITE
TEXT 		The name or identification number of a given site at which samples were collected.
LATITUDE
NUMBER 		The latitude of the sampling site in decmal degrees. Units for values are decimal degrees.
LONGITUDE
NUMBER 		The longitude of the sampling site in decimal degrees. Units for values are decimal degrees.
DATE
DATE 		The date (local time) on which as sample was collected.
TIME
TIME 		The time (local time) on the date in which a sample began to be collected.
SAMPLEID
TEXT 		The name or identification number of a individual samples collected at specific sites. IDs incorporate a 2 letter site code followed by the eight digit sampling date and a 2 digit code signifying the sample type.
OA
TEXT 		The concentration of okadaic acid measured in a sample. Units for values are micrograms per 100 grams of tissue.
DTX-1
TEXT 		The concentration of dinophysis toxin 1 measured in a sample. Units for values are micrograms per 100 grams of tissue.
DTX-2
TEXT 		The concentration of dinophysis toxin 2 measured in a sample. Units for values are micrograms per 100 grams of tissue.
AZA-1
TEXT 		The concentration of azaspiracid 1 measured in a sample. Units for values are micrograms per 100 grams of tissue.
AZA-2
TEXT 		The concentration of azaspiracid 2 measured in a sample. Units for values are micrograms per 100 grams of tissue.
AZA-3
TEXT 		The concentration of azaspiracid 3 measured in a sample. Units for values are micrograms per 100 grams of tissue.
Total OA equiv.
TEXT 		The sum of Okadaic acid, Dinophysis toxin 1 and Dinophysis toxin 2 for a given sample after equivalency factors have been applied. Units for values are micrograms per 100 grams of tissue.
PP2A
TEXT 		Result of the protein phosphatase 2A screening assay. Units for values are micrograms per 100 grams of tissue.
Shellfish Analysis Notes
TEXT 		Notes regarding the analyses of specific shellfish samples.

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Item Identification

Title: results from liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) from shellfish samples collected for lipophilic marine toxin analyses from the coast of Washington and Puget Sound from 2016-02-03 to 2016-12-20
Short Name: AZA Project Shellfish Data for Lipophilic Toxins In Washington State 2016
Status: Planned
Abstract:

Site names, coordinates, dates, and times that shellfish samples were collected for lipophilic marine toxin analyses. The results liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) are included. Additionally, the results of a screening assay for lipophilic toxins (PP2A) that detects okadaic acid and the dinophysis toxins are included.

Entity Information

Entity Type: Spreadsheet
Active Version?: Yes
Schema Name: PARR
Description:

Site names, coordinates, dates, and times that shellfish samples were collected for lipophilic marine toxin analyses. The results liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) are included. Additionally, the results of a screening assay for lipophilic toxins (PP2A) that detects okadaic acid and the dinophysis toxins are included.

Data Attributes

Attribute Summary

Rubric Score Primary Key? Name Type Description
100
 SITE TEXT The name or identification number of a given site at which samples were collected.
100
 LATITUDE NUMBER The latitude of the sampling site in decmal degrees. Units for values are decimal degrees.
100
 LONGITUDE NUMBER The longitude of the sampling site in decimal degrees. Units for values are decimal degrees.
100
 DATE DATE The date (local time) on which as sample was collected.
100
 TIME TIME The time (local time) on the date in which a sample began to be collected.
100
 SAMPLEID TEXT The name or identification number of a individual samples collected at specific sites. IDs incorporate a 2 letter site code followed by the eight digit sampling date and a 2 digit code signifying the sample type.
100
 OA TEXT The concentration of okadaic acid measured in a sample. Units for values are micrograms per 100 grams of tissue.
100
 DTX-1 TEXT The concentration of dinophysis toxin 1 measured in a sample. Units for values are micrograms per 100 grams of tissue.
100
 DTX-2 TEXT The concentration of dinophysis toxin 2 measured in a sample. Units for values are micrograms per 100 grams of tissue.
100
 AZA-1 TEXT The concentration of azaspiracid 1 measured in a sample. Units for values are micrograms per 100 grams of tissue.
100
 AZA-2 TEXT The concentration of azaspiracid 2 measured in a sample. Units for values are micrograms per 100 grams of tissue.
100
 AZA-3 TEXT The concentration of azaspiracid 3 measured in a sample. Units for values are micrograms per 100 grams of tissue.
100
 Total OA equiv. TEXT The sum of Okadaic acid, Dinophysis toxin 1 and Dinophysis toxin 2 for a given sample after equivalency factors have been applied. Units for values are micrograms per 100 grams of tissue.
100
 PP2A TEXT Result of the protein phosphatase 2A screening assay. Units for values are micrograms per 100 grams of tissue.
100
 Shellfish Analysis Notes TEXT Notes regarding the analyses of specific shellfish samples.

Attribute Details

SITE

CC ID: 797642
Seq. Order: 1
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The name or identification number of a given site at which samples were collected.
General Data Type: TEXT
Allowed Values: As provided

LATITUDE

CC ID: 797643
Seq. Order: 2
Data Storage Type: NUMBER
Required: No
Primary Key: No
Status: Active
Description:

The latitude of the sampling site in decmal degrees. Units for values are decimal degrees.
General Data Type: NUMBER
Unit of Measure: decimal degrees
Allowed Values: As provided

LONGITUDE

CC ID: 797644
Seq. Order: 3
Data Storage Type: NUMBER
Required: No
Primary Key: No
Status: Active
Description:

The longitude of the sampling site in decimal degrees. Units for values are decimal degrees.
General Data Type: NUMBER
Unit of Measure: decimal degrees
Allowed Values: As provided

DATE

CC ID: 797645
Seq. Order: 4
Data Storage Type: DATE
Required: No
Primary Key: No
Status: Active
Description:

The date (local time) on which as sample was collected.
General Data Type: DATE
Allowed Values: As provided

TIME

CC ID: 797646
Seq. Order: 5
Data Storage Type: TIME
Required: No
Primary Key: No
Status: Active
Description:

The time (local time) on the date in which a sample began to be collected.
General Data Type: TIME
Allowed Values: As provided

SAMPLEID

CC ID: 797647
Seq. Order: 6
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The name or identification number of a individual samples collected at specific sites. IDs incorporate a 2 letter site code followed by the eight digit sampling date and a 2 digit code signifying the sample type.
General Data Type: TEXT
Allowed Values: As provided

OA

CC ID: 797648
Seq. Order: 7
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The concentration of okadaic acid measured in a sample. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

DTX-1

CC ID: 797649
Seq. Order: 8
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The concentration of dinophysis toxin 1 measured in a sample. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

DTX-2

CC ID: 797650
Seq. Order: 9
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The concentration of dinophysis toxin 2 measured in a sample. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

AZA-1

CC ID: 797651
Seq. Order: 10
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The concentration of azaspiracid 1 measured in a sample. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

AZA-2

CC ID: 797652
Seq. Order: 11
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The concentration of azaspiracid 2 measured in a sample. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

AZA-3

CC ID: 797653
Seq. Order: 12
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The concentration of azaspiracid 3 measured in a sample. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

Total OA equiv.

CC ID: 797654
Seq. Order: 13
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

The sum of Okadaic acid, Dinophysis toxin 1 and Dinophysis toxin 2 for a given sample after equivalency factors have been applied. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

PP2A

CC ID: 797655
Seq. Order: 14
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

Result of the protein phosphatase 2A screening assay. Units for values are micrograms per 100 grams of tissue.
General Data Type: TEXT
Unit of Measure: micrograms per 100 grams of tissue
Allowed Values: less than the limit of detection to the measured value

Shellfish Analysis Notes

CC ID: 797656
Seq. Order: 15
Data Storage Type: TEXT
Required: No
Primary Key: No
Status: Active
Description:

Notes regarding the analyses of specific shellfish samples.
General Data Type: TEXT
Allowed Values: As provided

Catalog Details

Catalog Item ID: 54713
GUID: gov.noaa.nmfs.inport:54713
Metadata Record Created By: Jeffrey W Cowen
Metadata Record Created: 2018-11-08 11:33+0000
Metadata Record Last Modified By: SysAdmin InPortAdmin
Metadata Record Last Modified: 2022-08-09 17:11+0000
Metadata Record Published: 2018-11-08
Owner Org: NWFSC
Metadata Publication Status: Published Externally
Do Not Publish?: N
Metadata Last Review Date: 2018-11-08
Metadata Review Frequency: 1 Year
Metadata Next Review Date: 2019-11-08